Microstructural refinement of tantalum for Nb3Sn superconductor diffusion barriers
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abstract
Cast pure Ta was deformation processed via equal channel angular extrusion and then recrystallized to produce a uniform, fine-grained bulk material. Extrusions were performed on 2525150 mm billets at room temperature in 90 tooling to strains of 9.3. The Vickers microhardness reaches near maximum levels after four extrusions. As-worked microstructures are composed of nonuniform submicron grains with apparent banding. A homogeneous and fine grained recrystallized microstructure (average grain size 8 m) free of banding is obtained after four extrusions via route E multipass processing and a 1000C heat treatment. The high microstructural homogeneity of such a material may exhibit better co-reduction characteristics with surrounding Cu over conventionally processed Ta for superconductor diffusion barrier applications. 2005 IEEE.