Preparation of 5-and 6-carboxyfluorescein Academic Article

abstract

• Condensation of resorcinol with 4-carboxyphthalic anhydride in methanesulfonic acid gave a mixture of 5- and 6-carboxyfluorescein stereoisomers. These were separated by recrystallization from methanol- or ethanol-hexane to give 5- and 6-carboxyfluorescein, each in over 98% purity.

authors

• Burgess, Kevin

published proceedings

• SYNTHESIS-STUTTGART

altmetric score

• 9

author list (cited authors)

• Ueno, Y., Jiao, G. S., & Burgess, K.

citation count

• 21

complete list of authors

• Ueno, Y||Jiao, GS||Burgess, K

publication date

• October 2004

publisher

• Thieme  Publisher

published in

• Synthesis  Journal

keywords

• Chromophores
• Condensation
• FLUORESCENCE
• Heterocycles
• Regioselectivity

Digital Object Identifier (DOI)

• 10.1055/s-2004-829194

start page

• 2591

end page

• 2593

volume

• 2004

issue

• 15

URL

• http://dx.doi.org/10.1055/s-2004-829194