PREPARATION OF SOME CYCLIC FLUOROSILANES
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Fluorination with SbF3 has been used to prepare 1,1-difluoro-1-sitlacyclopent-3-ene, 1,1-difluoro-1-silacyclopen-2-ene, 1,1-difluoro-1-silacyclopen entane and a mixture of 1,1-difluoro-2-chloro-1-silacyclopentane and its 3-chloro isomer from the appropriate chlorosilanes. IR and NMR spectra of the products are reported. 1971.