4-METHYL-1,4-THIABORIN, AN AROMATIC BORON-SULFUR HETEROCYCLE
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The base-catalyzed hydrostannation of diethynyl sulfide with dibutylstannane affords 4,4-dibutyl-1,4-thiastanniny which reacts with methylboron dibromide to give 4-methyl-1,4-thiaborin. The thiaborin has been converted to tricarbonyl(6-4-methyl-1,4-thiaborin)molybdenum, which has been characterized by singlecrystal X-ray diffraction. 1995, American Chemical Society. All rights reserved.