71Ga and31P solid state NMR: A powerful tool for the characterization of the first gallium phosphonates
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abstract
Two new gallium phosphonates Ga(OH)(O3PC2H4-CO2H)-H2O 1 and Ga3(OH)3(O3PC2H4CO 2)22H2O 2 are prepared and characterized, using 31P MAS and 71Ga static NMR spectroscopy, showing a good correspondence between the fitted NMR parameters and the crystallographic data.