High pressure liquid chromatographic determination of zearalenone in chicken tissues. Academic Article

abstract

• A method is reported for the extraction and analysis of zearalenone in chicken fat, heart muscle, and kidney tissue by using high pressure liquid chromatography (HPLC). Zearalenone is extracted with acetonitrile, cleaned up with hexane, and extracted further with ethyl acetate. Zearalenone is determined by HPLC using a reverse phase radial compression separation system, an ultraviolet absorbance detector, and a mobile phase of acetonitrile-water (60 + 40) (v/v). Recoveries of zearalenone added at levels from 50 to 200 ng/g are in the range 82.6-95.1%.

authors

• Phillips, Timothy

published proceedings

• J Assoc Off Anal Chem

author list (cited authors)

• Turner, G. V., Phillips, T. D., Heidelbaugh, N. D., & Russell, L. H.

citation count

• 16

complete list of authors

• Turner, GV||Phillips, TD||Heidelbaugh, ND||Russell, LH

publication date

• January 1983

publisher

• Oxford University Press (OUP)  Publisher

published in

• Journal - Association of Official Analytical Chemists  Journal

keywords

• Adipose Tissue
• Animals
• Chickens
• Chromatography, High Pressure Liquid
• Kidney
• Myocardium
• Resorcinols
• Zearalenone

PubMed Central ID

• 6219097

Digital Object Identifier (DOI)

• 10.1093/jaoac/66.1.102

start page

• 102

end page

• 104

volume

• 66

issue

• 1

URL

• http://dx.doi.org/10.1093/jaoac/66.1.102