A high pressure liquid chromatographic method for the analysis of zearalenone in chicken blood
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A high pressure liquid chromatographic (HPLC) method is described to determine zearalenone in chicken blood. Samples are extracted with acetonitrile, followed by a hexane cleanup procedure and extracted further with ethyl acetate. The analysis of zearalenone is by HPLC using a reverse phase radial compression separation system, an ultraviolet absorbance detector and a mobile phase of acetonitrile-water 60:40 (v/v). Recoveries of zearalenone in blood at levels of 50-200 ng/ml are in the range of 66.8-72.6%.
author list (cited authors)
Turner, G. V., Phillips, T. D., Heidelbaugh, N. D., & Russell, L. H.
complete list of authors
Turner, GV||Phillips, TD||Heidelbaugh, ND||Russell, LH