Comparative studies of phase-cycling schemes for multiple pi-pulse sequences. Academic Article

abstract

• Recently, a new phase cycling scheme was introduced by this laboratory for use in biological solid-state NMR experiments involving multiple pi-pulses with characteristics that suggested it may enhance the sensitivity of these kind of experiments (Y. Li and J. N. S. Evans, 1995, Chem. Phys. Lett. 241, 79 and Erratum, 1995, ibid. 246, 527; Y. Li and J. N. S. Evans, 1996, J. Magn. Reson. B 111, 296). The new sequence followed the supercycled concept proposed a decade ago for heteronuclear decoupling experiments. In this paper, more detailed experiments demonstrate that the claim of enhanced sensitivity was unfounded, and in fact the supercycle proposed differs little from the established XY-8 and XY-16 based supercycles.

authors

• Igumenova, Tatyana

published proceedings

• J Magn Reson

author list (cited authors)

• Igumenova, T. I., Mitchell, D. J., & Evans, J. N.

citation count

• 5

complete list of authors

• Igumenova, TI||Mitchell, DJ||Evans, JN

publication date

• August 1997

publisher

• Elsevier  Publisher

published in

• Journal of Magnetic Resonance  Journal

keywords

• Magnetic Resonance Spectroscopy

PubMed Central ID

• 9281477

Digital Object Identifier (DOI)

• 10.1006/jmre.1997.1207

start page

• 144

end page

• 146

volume

• 127

issue

• 2

URL

• http%3A%2F%2Fdx.doi.org%2F10.1006%2Fjmre.1997.1207