PREPARATION AND X-RAY CRYSTAL-STRUCTURE OF BIS(PYRIDINIUM)-MU-DICHLORO-MU-OXO-TETRACHLORODIANTIMONATE(III) - DISCRETE ANTIMONY(III) OXYCHLORO-ANION
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abstract
Partial hydrolysis of the polymeric (pyH)3Sb2Cl 9 (py = pyridine) in ethanol leads to (pyH)2Sb 2OCl6 which is shown by X-ray crystallography to contain a discrete oxychloroanion of antimony(III) consisting of two octahedral :SbOCl4 units sharing a face.